边界润滑膜的微观分析

利用X—射线光电子能谱、扫描电镜等手段对新研制的含S、O、Mo油溶性化合物作为极压剂所形成的边界润滑膜进行了微观分析。结果表明:该极压剂的极压抗磨作用除了与极压剂在摩擦表面上分解,生成具有良好润滑性能的MoS_2、MoO_3、MoO_2等化合物有关外,还与极压剂对摩擦表面有化学抛光作用有关。     

利用 Nernst 效应的高 Tc 超导红外探测器分析

高T_c超导膜中Nernst效应的存在为研制辐射探测器开辟了新的途径。本文分析了以Nernst效应为基础的高T_c超导红外探测器的工作原理及有关的噪声源。     

溶胶一凝胶法制备二氧化钛及其转化为氮化钛的研究

本文以钛酸丁酯为原料，通过溶胶一凝胶法制备了ＴｉＯ２凝胶，在高温下烧结此凝胶得到ＴｉＯ２。将ＴｉＯ２粉末在９００°Ｃ以上用氨进行氮化，制得金黄色的氮化钛。通过使用热分析、色谱分析、扫描电镜及Ｘ一射线衍射等手段，研究并揭示了凝胶在陶瓷化生成ＴｉＯ２的过程中的化学反应，结晶及晶型随温度的变化规律。发现了氮化钛陶瓷的生成率与ＴｉＯ２溶胶的制备条件之间的关系。     

基于随机冲击的相关竞争失效可靠性评估

针对电子产品在工程实践中受随机冲击应力的影响及多失效模式的问题,以累积冲击和极限冲击来描述产品的冲击过程,考虑失效模式相关性并建立了随机冲击下产品竞争失效模型。以具有自然耗损和突发耗损特点金属化膜脉冲电容器为对象,进行了可靠性对比分析,验证了模型的合理性和有效性,为遭受复合应力影响的电子产品的可靠性评估提供了一种新方法。     

Al-Mn 多层膜离子束混合

离子束混合是一种材料改性和新材料研制的有效方法,本实验用Ａｒ＋离子束对Ａｌ－Ｍｎ多层薄膜在室温下进行轰击使其非晶化,并对样品电阻率随离子注入剂量及温度的变化关系进行原位测量．电阻温度系数ＴＣＲ和ＴＥＭ观测证实了样品离子束混合后电性能和结构发生改变生成了非晶相．     

微槽平板热管传热性能的实验研究

系统地研究小充液率条件下重力对微槽平板热管传热性能的影响,分析了工作温度、冷却方式等影响因素.发现重力对热管径向液膜的分布影响比较小,而对轴向的影响比较明显,从而使得倾角较大地影响了热管的传热能力.进一步证明了深槽平板热管具有良好的传热性能.     

Buckling analysis of embedded graphene oxide powder-reinforced nanocomposite shells

In this study, the buckling analysis of a Graphene oxide powder reinforced (GOPR) nanocomposite shell is investigated. The effective material properties of the nanocomposite are estimated through Halpin-Tsai micromechanical scheme. Three distribution types of GOPs are considered, namely uniform, X and O. Also, a first-order shear deformation shell theory is incorporated with the principle of virtual work to derive the governing differential equations of the problem. The governing equations are solved via Galerkin's method, which is a powerful analytical method for static and dynamic problems. Comparison study is performed to verify the present formulation with those of previous data. New results for the buckling load of GOPR nanocomposite shells are presented regarding for different values of circumfer-ential wave number. Besides, the influences of weight fraction of nanofillers, length and radius to thickness ratios and elastic foundation on the critical buckling loads of GOP-reinforced nanocomposite shells are explored.     

Experimental investigation for machinability aspects of graphene oxide/carbon fiber reinforced polymer nanocomposites and predictive modeling using hybrid approach

This article explores the drilling behavior of polymer nanocomposites reinforced by Graphene oxide/Carbon fiber using a hybrid method of Grey theory and Principal component analysis (GR-PCA). An online digital dynamometer was employed for the evaluation of Thrust Force and Torque. The image processing technique computes the delamination. Response surface methodology (RSM) considers the parameters, namely, drilling speed (S), feed rate (F), Graphene Oxide wt.% (G) in designing the experimentation array. Principal component analysis (PCA) was used to tackle the response priority weight during the combination of multiple functions. Analysis of variance (ANOVA) scrutinized the influence of parameters and intended the regression models to predict the response. GR-PCA evaluated the optimal parametric setting and remarked that feed rate acts as the most predominant factor. The higher feed rate and wt.% of G is responsible for surface damages like fiber pull-out, fiber fracture and cracks. A significant improvement in drilling responses has been obtained and also validates through confirmatory test and microstructure investigations.     

单[6-脱氧（1，10癸二硫醇）巯基]β-环糊精的合成方法研究

制备合成单[6-脱氧（1,10癸二硫醇）巯基]β-环糊精,结合产物的。^1H NMR,^13C HMR分析,推测了可能的反应机理,初步讨论了其在制备传感器敏感膜材料方面的应用前景。